OK, cool. much easier if you own the joint! ..and if you're not doing drums.
you're basically in the construction phase of the walls and such, the soundproofing part. Once you're done isolating yourself to the level you need then you go about treating the inside of the room for better acoustics with some traps, foam or curtains...
as far as the constuction specifics I'd ask here and go poke around the johnlsayers.com site for a couple days then come back here and get some acoustic advice, there you can find out about 703 insulation, Celotex(pressed soundboard you can buy at Home Depot) and installing the drywall screws(half schedule just means half as many).
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Kel
"is guitar your main instrument?" From an audience member at one of my gigs...